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http://148.72.244.84:8080/xmlui/handle/xmlui/3295| Title: | Synthesis and Characterizations of Silver Nano Particles using Chemical Reaction Method |
| Authors: | Khitam S. Shaker |
| Keywords: | Silver Nanoparticles Chemicals Reduction UV-Vie Absorption Spectra ABSTRACT In the present investigation colloidal silver nanoparticles was prepared by chemical reaction method from silver nitrate (AgNO3) and sodium citrate (Na3C6H5O7) in water. The preparation method were achieved at three levels of temperature (100, 150 and 200℃) the produced silver nanoparticles characterize by UV-vis Visible Spectroscopy, Scanning Electron Microscopy (SEM) and Particle Size analyzer the result of particle size analyzer show that their size distribution to lie in the range of (58.9 -202) nm. The results show that silver nanoparticles are 58.9, 76.4 and 202 nm at temperatures of (100, 150, 200) ℃, respectively can be produced. DOWNLOADS REFERENCES - Sepideh K. B., Kamyar Sh., Dayang R., Binti A. B. and Zurina Z. A., (2014), " Stirring Time Effect of Silver Nanoparticles Prepared in Glutathione Mediated by Green Method", Balavandy et al. Chemistry Central Journal , Vol.(8), 11. - Jong-S. K., (2007), "Reduction of Silver Nitrate in Ethanol by Poly (N-vinylpyrrolidone)", J. Ind. Eng. Chem., Vol. (13), No. 4, 566-570. - Burçak E., Elif Y., Sebahattin G., (2013), "Production of nanocrystalline silver particles by hydrogen reduction of silver nitrate aerosol droplets", Trans. Nonferrous Met. Soc. China, Vol. (23), 841−848. - Mercedes C. C., Gustavo R., Marcus W., Dominic H., Elza C.V.,Ralph S., Verónica B. R.,( 2015) " Plasma deposition of silver nanoparticles on ultrafiltration membranes: Antibacterial and anti-biofouling properties", Chemical Engineering Research and Design, Vol.(94), 524-537. -Wenning ., Lajun F., Hui F., Zhenzhen K., Meijuan G., (2011), "Ultrafine silver(II) oxide particles decorated porous ceramic composites for water treatment", Chemical Engineering Journal, Vol.(175), 592-599. - Javed I. H., Sunil K., Athar Adil H., Zaheer K., (2011), " Silver nanoparticles: preparation, characterization, and kinetics", Adv. Mat. Lett.,Vol. (2), No. 3, 188-194. - Raid S. J., Khalid F. S. and Ali H. Al- H., (2014)," Synthesis of Silver Nanoparticles", ARPN Journal of Engineering and Applied Sciences, Vol. (9), No. 4, 1819-6608 - Kamyar Sh., Mansor B. A., Mohsen Z., Wan M., Zin W. Y., Nor A. I. Parvaneh Sh., and Mansour Gh. M., ( 2011), "Synthesis and characterization of silver/montmorillonite/chitosan bionanocomposites by chemical reduction method and their antibacterial activity", Int J Nanomedicine., Vol. (6), 271–284. - Gopinath S. M., Niladri Sh. S., Jincy J. V., Noor S. Kh., Shyamil G., Ashwini P.G.M, (2013), ''Bilogical Synthesis, CHaracctrization and Application of Silver Nano particls- A Review", International Journal of Pharmaceuutical Applications, Vol. (4), 19-28. -Dr. Guo-Quan Lu, (2007), "Synthesis of Nano-Silver Colloids and Their Anti-Microbial Effects", Thesis, Blacksburg, Virginia, - Shan-Wei L., Shi-Hise C., Yen-Shang L., Chang-Cheng L., Chin-Min T., Yao-Chang L., Jui-Chang C. and Cheng-Liang H. (2014 ), " Effect of Temperature on the Growth of Silver Nanoparticles Using Plasmon-Mediated Method under the Irradiation of Green LEDs", Materials, Vol. (7), 7781-7798. - Lu, H.; Zhang, H.; Yu, X.; Zeng, S.; Yong, K.T.; Ho, H.P. (2012), "Seed-mediated plasmon-driven regrowth of silver nanodecahedrons (NDs)", Plasmonics,Vol. (7), 167–173. - Lee, Y.C.; Chen, S.J.; Huang, C.L., (2010), "Finding a facile method to synthesize decahedral silver nanoparticles through a systematic study of temperature effect on photomediated silver nanostructure growth", J. Chin. Chem. Soc., Vol. (57), 325–331. -Ratyakshi and Chauhan R.P., (2009), "Colloidal Synthesis of Silver Nano Particles",Asian Journal of Chemistry, Vol. (21), No. 10, S113-116. -Zhao, P., et al. (2013), "State of the art in gold nanoparticle synthesis" Coordination Chemistry Reviews , Vol. (257), 638-665. |
| Issue Date: | 2016 |
| Publisher: | University of Diyala – College of Engineering |
| Citation: | https://djes.info/index.php/djes |
| Abstract: | In the present investigation colloidal silver nanoparticles was prepared by chemical reaction method from silver nitrate (AgNO3) and sodium citrate (Na3C6H5O7) in water. The preparation method were achieved at three levels of temperature (100, 150 and 200℃) the produced silver nanoparticles characterize by UV-vis Visible Spectroscopy, Scanning Electron Microscopy (SEM) and Particle Size analyzer the result of particle size analyzer show that their size distribution to lie in the range of (58.9 -202) nm. The results show that silver nanoparticles are 58.9, 76.4 and 202 nm at temperatures of (100, 150, 200) ℃, respectively can be produced. |
| URI: | http://148.72.244.84:8080/xmlui/handle/xmlui/3295 |
| ISSN: | 1999-8716 |
| Appears in Collections: | مجلة ديالى للعلوم الهندسية / Diyala Journal of Engineering Sciences (DJES) |
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| File | Description | Size | Format | |
|---|---|---|---|---|
| KHITAM 9.pdf | 1.07 MB | Adobe PDF | View/Open |
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